交联羟丙基羧甲基木薯淀粉性质的研究
详细信息Study on properties of cross-linking hydroxypropyl carboxymethyl starch
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摘要: 对交联羟丙基羧甲基木薯淀粉(CHMS)的白度、糊粘度、透明度、冻融稳定性、耐盐性进行了测定,并利用红外光谱(FT-IR)对交联羟丙基羧甲基木薯淀粉结构进行了表征。结果表明,经过复合变性的淀粉白度下降至90.1%,而冷糊粘度升高至925mPa·s,糊透光率升高至70.7%,冻融稳定性、耐盐性也得到改善;红外谱图显示了各特征基团的特征吸收峰,证实了其分子基团的变化。对木薯淀粉进行交联羟丙基羧甲基复合变性,有利于提高其在工业中的应用价值。Abstract: The whiteness, paste viscosity, transparency, freeze-thaw stability and salt tolerance of cross-linking hydroxypropyl carboxymethyl starch (CHMS) were tested, and the molecule structure of CHMS was detected by FT-IR. Results showed that the cold paste viscosity was increased to 925mPa·s, the luminousness was up to 70. 7%, the freeze-thaw stability and salt tolerance of starch were also improved after been compound modified, while its whiteness was decreased to 90. 1%. New peaks were showed in the IR spectrogram, which proved the change of molecule groups of CHMS. Results above showed that, the preparation of CHMS could help to improve the value of tapioca starch in the industry.
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[1] Bhupinder K, Fazilah A, Rajeev B, et al.Progress in starch modification in the last decade[J].Food Hydrocolloids, 2011 (2) :1-7.
[2] Kyungsoo W, Paul A S.Cross-linking of wheat starch and hydroxypropylated wheat starch in alkaline slurry with sodium trimetaphosphate[J].Carbohydrate Polymers, 1997, 33:263-271.
[3] 李光磊, 王忠诚, 刘继华.羟丙基玉米淀粉的制备及特性研究[J].粮油食品科技, 2001, 9 (2) :7-9. [4] 张燕萍.变性淀粉制造与应用[M].北京:化学工业出版社, 2007:169. [5] Srivastava H C, Patel M M, Ahmedabad.Viscosity stabilization of tapioca starch[J].Starch-Strke, 1973, 29 (1) :17-21.
[6] 张筱璐, 万冰清, 刘丽丽, 等.溶剂法制备高粘度羧甲基淀粉[J].华东理工大学学报, 2007, 33 (3) :365-368. [7] 杨玉玲, 周凤娟, 李新华.交联-羧甲基复合变性淀粉的制备及性能研究[J].中国粮油学报, 2001, 16 (6) :47-50. [8] 徐忠, 张亚丽.马铃薯羧甲基淀粉的理化性质及结构分析研究[J].黑龙江商学院学报, 2000, 16 (4) :7-12. [9] 孙慧敏, 马晓军.木薯淀粉及木薯变性淀粉性质比较研究[J].食品工业科技, 2008, 29 (6) :82-87. [10] 江雄知.交联羧甲基木薯淀粉的合成与动力学研究[D].桂林:桂林理工大学, 2009. [11] 刘松青, 杨婉身, 张祖民, 等.马铃薯羟丙基羧甲基淀粉颗粒及分子结构变化[J].中国粮油学报, 2010, 25 (1) :44-46. [12] 王布强, 陈祥贵, 袁怀波, 等.交联羧甲基复合变性木薯淀粉的制备及性质[J].食品科学, 2008, 29 (10) :178-182. [13] 刘松青.马铃薯原淀粉制备羟丙基羧甲基淀粉新型片剂辅料的研究[D].雅安:四川农业大学, 2007. [14] Wang L F, Pan S Y, Hu H, et al.Synthesis and properties of carboxymethyl kudzu root starch[J].Carbohydrate Polymers, 2010, 80:174-179.
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