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亚临界流体萃取崖柏挥发油及其成分分析

张育光, 侯春, 吴新星, 姜兴涛, 余汉谋, 李剑政

张育光, 侯春, 吴新星, 姜兴涛, 余汉谋, 李剑政. 亚临界流体萃取崖柏挥发油及其成分分析[J]. 食品工业科技, 2015, (21): 210-213. DOI: 10.13386/j.issn1002-0306.2015.21.035
引用本文: 张育光, 侯春, 吴新星, 姜兴涛, 余汉谋, 李剑政. 亚临界流体萃取崖柏挥发油及其成分分析[J]. 食品工业科技, 2015, (21): 210-213. DOI: 10.13386/j.issn1002-0306.2015.21.035
ZHANG Yu-guang, HOU Chun, WU Xin-xing, JIANG Xing-tao, YU Han-mou, LI Jian-zheng. Extraction of the Thuja sutchuenensis essential oil by sub-critical fluid extraction technology and its component analysis[J]. Science and Technology of Food Industry, 2015, (21): 210-213. DOI: 10.13386/j.issn1002-0306.2015.21.035
Citation: ZHANG Yu-guang, HOU Chun, WU Xin-xing, JIANG Xing-tao, YU Han-mou, LI Jian-zheng. Extraction of the Thuja sutchuenensis essential oil by sub-critical fluid extraction technology and its component analysis[J]. Science and Technology of Food Industry, 2015, (21): 210-213. DOI: 10.13386/j.issn1002-0306.2015.21.035

亚临界流体萃取崖柏挥发油及其成分分析

详细信息
    作者简介:

    张育光 (1969-) , 男, 大专, 从事烟草卷烟研究, E-mail:htyg@hongta.com。 ;

    侯春 (1973-) , 男, 硕士, 工程师, 主要从事香精香料领域、香料工程与化学等研究, E-mail:houchun@hongta.com。;

  • 中图分类号: TQ914;TQ028.32

Extraction of the Thuja sutchuenensis essential oil by sub-critical fluid extraction technology and its component analysis

  • 摘要: 崖柏挥发油有良好的生物活性。为了优化崖柏挥发油的萃取条件,以二甲醚为萃取剂,采用亚临界流体萃取技术萃取崖柏挥发油,并对萃取条件包括萃取温度、萃取时间、萃取次数进行优化,用GC-MS对所得的崖柏挥发油进行了成分分析。结果表明,亚临界流体萃取崖柏挥发油的最佳条件为:萃取温度为40℃,萃取次数3次,每次萃取时间30 min,在此条件下崖柏挥发油的提取率为6.3%。GC-MS分析显示崖柏挥发油的主要成分罗汉柏烯和α-柏木脑,分别占挥发油的34.74%,20.09%。利用亚临界流体萃取技术能高效的萃取崖柏挥发油。 
    Abstract: The Thuja sutchuenensis essential oil has good biological activity. In order to optimize the extraction conditions, it was extracted by sub- critical fluid extraction technology, choosing DME as extracting agent. The extraction temperature, extraction time, extraction times was investigated. The results showed that the optimal conditions of subcritical fluid extraction of Thuja sutchuenensis were as follows: 40 ℃ for extracting 30 min, 3 times.Under those conditions, the extraction rate was up to 6.3%. The essential oil components were separated and identified by GC- MS. Thujopsene, α- cedorl were the main components, accounting for 34.74%, 20.09% of the Thuja sutchuenensis Essential oil respectively.Sub- critical fluid extraction technolongy could efficiently extract the Thuja sutchuenensis essential oil.
  • [1] 中国科学院中国植物志编委会.中国植物志[J].北京:科学出版社, 1978, 26:318.
    [2] 郭泉水, 王祥福, 巴哈尔古丽, 等.崖柏群落优势乔木树种种间关系[J].生态学杂志, 2007, 26 (12) :1911-1917.
    [3] 郑群明, 吴楚材, 谭益民, 等.崖柏乙醇提取物抑菌作用的初步研究[J].中南林业科技大学学报, 2011, 31 (4) :66-69.
    [4] 袁昌齐, 肖正春.世界植物药[M].南京:东南大学出版社, 2013, 01.
    [5] 包秀萍, 刘煜宇, 普元柱, 等.亚临界流体萃取贡菊净油的方法及其成分分析[J].食品研究与开发, 2014, 35 (7) :100-103.
    [6] 李玲, 陈志强, 李修禄.超临界流体萃取法在中药材质量控制中的应用[J].药学学报, 1995, 30 (2) :133-137.
    [7] 胡爱军, 丘泰球, 梁汉华.超临界流体萃取强化技术及应用[J].精细化工, 2001, 18 (12) :736-740.
    [8] 刘月蓉, 牟大庆, 陈涵, 等.天然植物精油提取技术-亚临界流体萃取[J].莆田学院学报, 2011, 18 (2) :67-70.
    [9]

    Shalmashi A, Abedi M, Golmohamm a F, et al.Isolation of caffeine from tea waste using subcritical water extraction[J].Journal of Food Process Engineering, 2010, 33 (4) :701-711.

    [10]

    Hee J L, Min C K, Byung H, U.Determination of phyllodulcin from sweet hydrangea leaves by subcritical water extraction and high performance liquid chromatographic analysis[J].Journal of Liquid Chromatography&Related Technologies, 2008, 31 (9) :1306-1313.

    [11] 吴雪辉, 刘肖丽, 刘智锋, 等.油茶籽油亚临界流体粗爱去工艺及品质研究[J].中国油脂, 2012, 37 (10) :6-9.
    [12] 刘平怀, 时杰, 沈世军.亚临界流体萃取法回收废弃虾蟹壳中虾青素[J].精细化工, 2011, 28 (5) :497-500.
    [13] 卢杰, 刘思聪, 王兰, 等.响应面法优化亚临界流体萃取海带中叶绿素工艺[J].食品科技, 2012, 37 (12) :197-202.
    [14] 刘志明, 王海英, 王芳, 等.侧柏心材和树皮精油的GC-MS分析[J].西部林业科学, 2011, 40 (1) :26-29.
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  • 收稿日期:  2015-04-22

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