Research of solid fermentation technology of Zanthoxylum bungeanum liquor
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摘要: 以柠檬烯含量、芳樟醇含量和感官评分为指标,对花椒酒的固态发酵工艺进行研究,采用正交实验优化了工艺条件,并利用气相色谱-质谱法（GC-MS）进一步对花椒酒的风味成分进行分析鉴定。结果表明:红花椒适于花椒酒酿制,最佳酿造工艺条件为花椒用量0.4%、花椒粉碎度60目、酿造时间9 d,所得花椒酒中柠檬烯和芳樟醇分别为45.4 mg/L和39.8 mg/L,感官评分90分。柠檬烯、芳樟醇、月桂烯、乙酸芳樟酯、（-）-4-萜品醇、桉叶油醇、α-松油醇等与乙醇、正丙醇、叔丁醇、乙酸乙酯、异丁醇、异戊醇、乙缩醛等共同构成了花椒酒的典型风味。Abstract: The content of limonene and linalool,sensory evaluation as indexes,the brew technology of Zanthoxylum bungeanum liquor by solid fermentation was researched and the orthogonal test was designed to optimize the brew technology.The flavor compounds of Z. bungeanum liquor were further analyzed by gas chromatography-mass spectrometry( GC- MS).The results indicated that red Z.bungeanum was suitable for brewing Z.bungeanum liquor,the optimum process conditions were Z. bungeanum content 0.4%,particle size 60- mesh,brewage time 9days.Under the optimum condition,limonene was 45.4 mg / L,linalool was 39.8 mg / L in the Z. bungeanum liquor,sensory evaluation was 90. Zanthoxylum bungeanum contributed to limonene,linalool,linalyl acetate,(-)- 4-terpineol,cineole,etc and ethanol,1- propanol,tert- butanol,ethyl acetate,2- methyl-1- propanol,acetal,etc were fermented by microorganism.These compounds constituted typical flavor of Z.bungeanum liquor.
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Keywords:
- Zanthoxylum bungeanum liquor /
- solid fermentation /
- limonene /
- linalool /
- flavor compounds
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[1] 王宇,巨勇,王钊.花椒属植物中生物活性成分研究近况[J].中草药,2002,33(7):666-670. [2] 赵秀玲.花椒的化学成分、药理作用及其资源开发的研究进展[J].中国调味品,2012,37(3):1-5. [3] 袁娟丽,王四旺.花椒的化学成分及药效研究[J].现代生物医学研究进展,2010,10(3):552-554. [4] Liu S,Wei L.Analysis of volatile oil in pericarpium Zanthoxyli[J].China Journal of Chinese Materia Medica,1991,16(6):359-360,383.
[5] Quan Boxiong,Da Wenshi,Mizuo Mizuno.Flavonol glucosides in pericarps of Zanthoxylum bungeanum[J].Phytochemistry,1995,39(3):723-725.
[6] GONG Zhunan,MI Xianghui,LIANG Qiaoli,et al.Study on super-critical carbon dioxide extraction of volatile oil from Zanthoxylum bungeanum maxim.CV.Da Hongpao and its chemical components[J].International Journal of Epidemiology,2005,24(6):1147-1153.
[7] 薛婷,黄峻榕,李宏梁.国内外花椒副产物的研究现状及其发展趋势[J].中国调味品,2013,38(12):106-110. [8] Shuai Huang,Lei Zhao,Xian Li Zhou,et al.New alkylamides from pericarps of Zanthoxylum bungeanum[J].Chinese Chemical Letters,2012,23(11):1247-1250.
[9] Tirillini B,Manunta A,Am S.Constituents of the Essential Oil of the Fruits of Zanthoxylum bungeanum[J].Planta Medica,1991,57(1):90-91.
[10] 吴建平.小曲白酒酿造法[M].北京:中国轻工业出版社,1995:73-109. [11] 罗凯,朱琳,阚建全.气相色谱法测定不同产地花椒挥发油中芳樟醇和柠檬烯含量的研究[J].中国粮油学报,2012,27(8):119-123. [12] 范文来,胡光源,徐岩.顶空固相微萃取-气相色谱-质谱法测定药香型白酒中萜烯类化合物[J].食品科学,2012,33(14):110-116. [13] 杨建刚,吴赫川,周健,等.基于顶空固相微萃取技术结合气相色谱质谱联用法的川法小曲白酒挥发性成分研究[J].食品安全检测学报,2015,6(7):2666-2679. [14] GUO Z A,ZHAO J C,XIE Z H.Study on chemical constituents of the essential oil from Zanthoxylum Bungeanum Maxim by gas chromatography-mass spectrometry[J].Journal of Chromatography,2003,19(6):567-568.
[15] 李大和.白酒酿造培训教程[M].北京:中国轻工业出版社,2013:479-515. [16] 罗凯,朱琳,阚建全,等.不同产地青花椒和红花椒挥发油的比较研究[J].食品工业科技,2012,33(18):103-106. [17] 杨峥,公敬欣,张玲,等.汉源红花椒和金阳青花椒香气活性成分研究[J].中国食品学报,2014,14(5):226-230. [18] Susanne Kern,Thierry Granier,Hafida Dkhil,et al.Stability of limonene and monitoring of a hydroperoxide in fragranced products[J].Flavour and Fragrance Journal,2014,29(5):277-286.
[19] Michael J Calandra,John Impellizzeri,Ying Wang.An HPLC method for hydroperoxides derived from limonene and linalool in citrus oils,using post-column luminol-mediated chemiluminescence detection[J].Flavour and Fragrance Journal,2015,30(2):121-130.
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